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(Fig. 4.18). However, none of the polymer systems suggested to date seems to have used more than tridentate ligands. Examples of research progress over the past few years include a number of electropolymerization studies by Meyer. For example, poly[4-(2-aminoethyl)styrene], prepared by living anionic polymerization with about 18 repeat units has been derivatized by amide coupling to [RuII (4-vinyl-40 -methyl-2,20 -bipyridine)2 (4-methyl-2,20 -bipyridine-40 carboxylic acid)]2C . The product PS-[(CH2 CH2 NHCO-bpy-4-methyl)(4-vinyl-40 methyl-2,20 -bipyridine)2 RuII ]36C undergoes reductive electropolymerization (at 18 the vinyl groups Type III type) and gives open porous lms that appear to retain the electron-transfer and excited-state properties of the original ruthenium species slightly modi ed by the lm (104). A number of related Type III species have also been investigated by Meyer and others as well (105 107). Two examples and an energy-minimized structure for one of the anchored ruthenium(II) species are shown in Figure 4.19. Also, the potential applications of chiral ruthenium(II) polymers to induce chiral photosynthesis and to provide optically active luminescence have brought forth new chiral ruthenium coordination polymers. As noted in 3, stereoselective condensation reactions between - and -bis(1,10phenanthroline-5,6-dione)bipyridineruthenium(II) ions and - and -bis(1,10phenanthroline-5,6-diamine)bipyridineruthenium(II) ions produces homochiral - and -coordination polyelectrolytes and a meso , -coordination polyelectrolyte (Fig. 4.20) (108). Tor and Glaser have also prepared chiral ruthenium(II) polyelectrolytes (109), and a review article on this synthetic concept for ruthenium(II) oligomers from dimers to decamer dendrimers has appeared (110). asp.net qr code reader QR Code Scanner in ASP.Net - CodeProject
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